triethylamine in dichloromethane

lithium aluminium tetrahydride in diethyl ether 1.) reflux, 3 h; 2.) room temperature, 14 h;

in diethyl ether

1: 1.) yellow mercuric oxide; 2.) hydchloric acid / 1.) aq. acetic acid; 2.) water 2: 100 percent / LiAlH4 / diethyl ether / 1.) reflux, 3 h; 2.) room temperature, 14 h View Scheme

1.1: nitric acid; bromine / 16.25 h / 20 - 70 °C 2.1: sodium hydroxide; mercury(II) oxide; acetic acid / water / 72 h / Heating; Reflux 2.2: pH ~ 1 3.1: diethyl ether 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C View Scheme

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