2,2,4,4-四甲基-3-戊酮肟合成路线 （共 14 条）
反应条件
N,O-bis(trimethylsilyl)hydroxylamine; potassium hydride in tetrahydrofuran 15 h; Heating- 78 deg C to room temp.;
参考文献
Hoffman, Robert V.; Buntain, Gregory A.
Synthesis, 1987 , # 9 p. 831 - 833
反应条件
hydroxylamine hydrochloride; sodium acetate in ethanol
参考文献
Bordwell; Zhang, Shizbong
Journal of the American Chemical Society, 1995 , vol. 117, # 17 p. 4858 - 4861
反应条件
1: 77 percent / Na / hexane / 1.5 h 2: 88 percent / NH2OH*HCl / methanol / 3.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 7 p. 2050 - 2053
参考文献
Eisenhauer, Brian M.; Wang, Minghui; Labaziewicz, Henryk; Ngo, Maria; Mendenhall, G. David
Journal of Organic Chemistry, 1997 , vol. 62, # 7 p. 2050 - 2053
反应条件
T=20°C; 90 h; Title compound not separated from byproducts;
参考文献
Coseri, Sergiu; Mendenhall, G. David; Ingold
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4629 - 4636
反应条件
T=20°C; 90 h; Title compound not separated from byproducts;
参考文献
Coseri, Sergiu; Mendenhall, G. David; Ingold
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4629 - 4636
反应条件
(i), (ii) NH2OH*HCl; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 95, p. 2963 - 2971
参考文献
Coseri, Sergiu; Mendenhall, G. David; Ingold
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4629 - 4636
反应条件
in benzene T=25°C; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 95, p. 8610 - 8614
反应条件
T=75°C; P=4854350 Torr; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 81, p. 2151,2153
