2-(二苄基氨基)乙酸乙酯合成路线 （共 12 条）
反应条件
in ethanol T=140°C; 0.333333 h; Microwave irradiation;
参考文献
Vitale, Romina; Ottonello, Giuliana; Petracca, Rita; Bertozzi, Sine Mandrup; Ponzano, Stefano; Armirotti, Andrea; Berteotti, Anna; Dionisi, Mauro; Cavalli, Andrea; Piomelli, Daniele; Bandiera, Tiziano; Bertozzi, Fabio
ChemMedChem, 2014 , vol. 9, # 2 p. 323 - 336
反应条件
in dichloromethane 2 h;
参考文献
Broxterman, H. J. G.; Liskamp, R. M. J.
Recueil des Travaux Chimiques des Pays-Bas, 1991 , vol. 110, # 2 p. 46 - 52
反应条件
3CO(1-)*Fe(3+)*NO(1-) in 1,2-dichloro-ethane T=60°C; 18 h; Inert atmosphere;
参考文献
Holzwarth, Michael S.; Alt, Isabel; Plietker, Bernd
Angewandte Chemie - International Edition, 2012 , vol. 51, # 22 p. 5351 - 5354
反应条件
1,5-bis-(diphenylphosphino)-pentane; copper diacetate; sodium hydrogencarbonate in N,N-dimethyl-formamide T=20°C; Inert atmosphere; Reagent/catalystSolventConcentration;
参考文献
Matsuda, Naoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Angewandte Chemie - International Edition, 2012 , vol. 51, # 47 p. 11827 - 11831
Angewandte Chemie, 2012 , vol. 124, # 47 p. 11997 - 12001
反应条件
1: TolS(O)CH2Cl With isopropylmagnesium chloride in tetrahydrofuran T=-78°C; 2: N-Benzylbenzylamine With n-butyllithium in tetrahydrofuran T=-78 - -40°C; 3: chloroformic acid ethyl ester in tetrahydrofuran T=-40°C;
参考文献
Satoh, Tsuyoshi; Osawa, Atsushi; Ohbayashi, Tohru; Kondo, Atsushi
Tetrahedron, 2006 , vol. 62, # 33 p. 7892 - 7901
反应条件
chlorine dioxide in acetonitrile 1 h; different pH's; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 47, # 5 p. 892 - 893
反应条件
chlorine dioxide in acetonitrile 1 h; different pH's; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 47, # 5 p. 892 - 893
反应条件
chlorine dioxide in acetonitrile 1 h; different pH's; Product distribution;
参考文献
Burrows, Elizabeth P.; Rosenblatt, David H.
Journal of Organic Chemistry, 1982 , vol. 47, # 5 p. 892 - 893
反应条件
trichloroethane, 1,1,2-; 10 palladium on activated carbon; hydrogen in methanol P=760.051 Torr; 1 h; chemoselective reaction;
参考文献
Cheng, Chuanjie; Sun, Jianwei; Xing, Lixin; Xu, Jimin; Wang, Xinyan; Hu, Yuefei
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5671 - 5674
反应条件
lithium diisopropyl amide 1.) THF/toluene/cyclohexane, -78 to -40 deg C 2.) -78 to 5 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Broxterman, H. J. G.; Liskamp, R. M. J.
Recueil des Travaux Chimiques des Pays-Bas, 1991 , vol. 110, # 2 p. 46 - 52
