N-(2-苯基乙基)苯磺酰胺合成路线 （共 12 条）
反应条件
sodium hydroxide man erhitzt das rohe Benzolsulfonsaeure-<methyl-β-phenaethylamid> mit konz.Salzsaeure af 150-160grad;
参考文献
Johnson; Guest
American Chemical Journal, 1909 , vol. 42, p. 346
反应条件
4-Methylpyridine in dichloromethane
T=20°C; 1 h;
参考文献
Chantarasriwong, Oraphin; Jang, Doo Ok; Chavasiri, Warinthorn
Tetrahedron Letters, 2006 , vol. 47, # 42 p. 7489 - 7492
反应条件
triethylamine; 1-(toluene-p-sulphonyl)imidazole in N,N-dimethyl-formamide
Reflux;
参考文献
Rad, Mohammad Navid Soltani; Behrouz, Somayeh; Nekoei, Abdo-Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2014 , vol. 189, # 4 p. 465 - 476
反应条件
triethylamine; benzenesulfonyl chloride in N,N-dimethyl-formamide
参考文献
CASTELLS BOLIART, JOSEP; MIGUEL CENTENO, David Enrique; PASCUAL GILABERT, Marta
Patent: US2012/122920 A1, 2012 ;
Title/Abstract Full Text Show Details
Castells Boliart, Josep; Miguel Centeno, David Enrique; Pascual Gilabert, Marta
Patent: US2012/149909 A1, 2012 ;
反应条件
dimethylsulfide borane complex in tetrahydrofuran
Ambient temperature;
参考文献
Belletire, J. L.; Fry, D. F.
Synthetic Communications, 1988 , vol. 18, # 1 p. 29 - 36
反应条件
Ir(III) chloride; potassium carbonate
T=150°C; 24 h;
参考文献
Liu, Chuanzhi; Liao, Shiheng; Li, Qiang; Feng, Sunlin; Sun, Qing; Yu, Xiaochun; Xu, Qing
Journal of Organic Chemistry, 2011 , vol. 76, # 14 p. 5759 - 5773
反应条件
in tetrahydrofuran
72 h; Ambient temperature;
参考文献
Katritzky; Zhang; Wu
Synthetic Communications, 1994 , vol. 24, # 2 p. 205 - 216
反应条件
1: 100 percent / Cl3CCN; PPh3 / CH2Cl2 / 1 h / Heating
2: 87 percent / 4-picoline / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Chantarasriwong, Oraphin; Jang, Doo Ok; Chavasiri, Warinthorn
Tetrahedron Letters, 2006 , vol. 47, # 42 p. 7489 - 7492
反应条件
1: 20 h / Sonication; Neat (no solvent)
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 20 °C
View Scheme
参考文献
Garcia Ruano, Jose L.; Parra, Alejandro; Marzo, Leyre; Yuste, Francisco; Mastranzo, Virginia M.
Tetrahedron, 2011 , vol. 67, # 16 p. 2905 - 2910
反应条件
1: sodium; alcohol
2: benzene; aqueous KOH-solution
View Scheme
参考文献
Johnson; Guest
American Chemical Journal, 1909 , vol. 42, p. 346
