N-(二苯基亚甲基)-1-苯甲胺合成路线 （共 34 条）
反应条件
1: palladium diacetate; Nixantphos; sodium hexamethyldisilazane / 3 h / 24 °C / |Inert atmosphere 2: hydrogenchloride / tetrahydrofuran; water / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Li, Minyan; Yuecel, Baris; Adrio, Javier; Bellomo, Ana; Walsh, Patrick J.
Chemical Science, 2014 , vol. 5, # 6 p. 2383 - 2391
反应条件
1: palladium diacetate; Nixantphos; sodium hexamethyldisilazane / 3 h / 24 °C / |Inert atmosphere 2: hydrogenchloride / tetrahydrofuran; water / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Li, Minyan; Yuecel, Baris; Adrio, Javier; Bellomo, Ana; Walsh, Patrick J.
Chemical Science, 2014 , vol. 5, # 6 p. 2383 - 2391
参考文献
Reddelien
Chemische Berichte, 1920 , vol. 53, p. 343;
Chemische Berichte, 1921 , vol. 54, p. 3125,3128,3129,3130
反应条件
1: sodium hydride / tetrahydrofuran; hexamethylphosphoric acid triamide 2: aq. H2SO4 / Ambient temperature 3: aq. H2SO4 / Ambient temperature View Scheme
参考文献
Armesto, Diego; Ortiz, Maria J.; Perez-Ossorio, Rafael
Tetrahedron Letters, 1981 , vol. 22, # 23 p. 2203 - 2206
反应条件
man kocht das entstehenden Jodmethylat mit Alkohol;
参考文献
Sommelet
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1927 , vol. 184, p. 1339,1500
反应条件
20 h; Heatingor irradiation;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 19, # 12 p. 1082 - 1083
反应条件
1: KOH, K2CO3, (1R,2S)-1-(diphenylmethyleneamino)-2-hydroxymethyl-1-methylpyrrolidinium iodide / CH2Cl2 / 24 h / Ambient temperature 2: 10percent aq. HCl / various solvent(s) / 16 h / 70 °C View Scheme
参考文献
Dehmlow, Eckehard Volker; Klauck, Robert; Duettmann, Stephanie; Neumann, Beate; Stammler, Hans-Georg
Tetrahedron Asymmetry, 1998 , vol. 9, # 13 p. 2235 - 2244
反应条件
4 Angstroem MS; [ReBr(CO)3(thf)]2 in toluene T=115°C; 24 h;
参考文献
Kuninobu, Yoichiro; Nishina, Yuta; Nakagawa, Chie; Takai, Kazuhiko
Journal of the American Chemical Society, 2006 , vol. 128, # 38 p. 12376 - 12377
反应条件
1: KOH, K2CO3, (1R,2S)-1-(diphenylmethyleneamino)-2-hydroxymethyl-1-methylpyrrolidinium iodide / CH2Cl2 / 24 h / Ambient temperature 2: 10percent aq. HCl / various solvent(s) / 16 h / 70 °C View Scheme
参考文献
Dehmlow, Eckehard Volker; Klauck, Robert; Duettmann, Stephanie; Neumann, Beate; Stammler, Hans-Georg
Tetrahedron Asymmetry, 1998 , vol. 9, # 13 p. 2235 - 2244
反应条件
in tetrahydrofuran T=25°C; Equilibrium constant;
参考文献
Antipin, I. S.; Vedernikov, A. N.; Solomonov, B. N.; Konovalov, A. I.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 101 p. 1861 - 1865
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 10 p. 2060 - 2065
