N-烯丙基-N,N-双(三甲基甲硅烷基)胺合成路线 (共 26 条)
反应条件
methyl iodide in Petroleum ether
26 h; Heating;
参考文献
Hamada, Yoshitaka; Yamamoto, Yasushi; Shimizu, Hideaki
Journal of Organometallic Chemistry, 1996 , vol. 510, # 1-2 p. 1 - 6
反应条件
1,1,1,3,3,3-hexamethyl-disilazane
T=0 - 20°C;
参考文献
Quirk, Roderic P.; Kim, Hoon; Polce, Michael J.; Wesdemiotis, Chrys
Macromolecules, 2005 , vol. 38, # 19 p. 7895 - 7906
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
Ambient temperature;
参考文献
Bruening, Joerg
Tetrahedron Letters, 1997 , vol. 38, # 18 p. 3187 - 3188
反应条件
n-butyllithium in hexane
96 h; Heating;
参考文献
Paulini, Klaus; Reissig, Hans-Ulrich
Liebigs Annalen der Chemie, 1991 , # 5 p. 455 - 461
反应条件
1,1,1,3,3,3-hexamethyl-disilazane
8 h; Ambient temperature;
参考文献
Bestmann, Hans Juergen; Woelfel, Gerhard
Chemische Berichte, 1984 , vol. 117, # 3 p. 1250 - 1254
参考文献
Ghose,B.N.
Journal of Organometallic Chemistry, 1979 , vol. 164, p. 11 - 18
反应条件
silver(I) in tetrahydrofuran
48 h; Ambient temperature;
参考文献
Murai, Toshiaki; Yamamoto, Mikio; Kato, Shinzi
Journal of the Chemical Society, Chemical Communications, 1990 , # 11 p. 789 - 790
反应条件
triethylamine; titanium tetrachloride
1) CH2Cl2, 45 min, r.t., 2) 4 h, reflux; Yield given. Multistep reaction;
参考文献
Schorr, Manfred; Schmitt, Wilfried
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 68, # 1-4 p. 25 - 36
反应条件
n-butyllithium; water
1.) THF, hexane, 0 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Corriu; Bolin; Moreau
Tetrahedron Letters, 1991 , vol. 32, # 33 p. 4121 - 4124
反应条件
1,1,1,3,3,3-hexamethyl-disilazane
8 h; Ambient temperature;
参考文献
Bestmann, Hans Juergen; Woelfel, Gerhard
Chemische Berichte, 1984 , vol. 117, # 3 p. 1250 - 1254