反应条件
1.1: sulfuric acid / 0 - 10 °C 2.1: sulfuric acid / 3 h / 80 °C 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 - 20 °C 4.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C 5.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C 5.2: 1 h / 0 - 5 °C 6.1: sodium hydroxide; water / methanol / 2 h / 70 °C 6.2: 0.5 h / 4 °C / pH 2 7.1: hydrogen / palladium 10 on activated carbon / methanol / 0.25 h / 2068.65 Torr View Scheme
参考文献
ORCHID RESEARCH LABORATORIES LTD.; RAJAGOPAL, Sridharan; THANGAPAZHAM, Selvakumar; PAUL-SATYASEELA, Maneesh; BALASUBRAMANIAN, Gopalan; SHAKTI SINGH, Solanki; KUPPUSAMY, Bharathimohan; KACHHADIA, Virendra; CHENNIAPPAN, Vinoth Kumar; GANESAN, Karthikeyan; NARAYANAN, Shridhar
Patent: WO2011/58582 A1, 2011 ;
WO 2011/058582 A1
