2,2,6,6-四甲基哌啶合成路线 (共 107 条)
反应条件
n-butyllithium in hexane; pentane
参考文献
Lappert, Michael F.; Slade, Martin J.; Singh, Anirudh; Atwood, Jerry L.; Rogers, Robin D.; Shakir, Riz
Journal of the American Chemical Society, 1983 , vol. 105, # 2 p. 302 - 304
反应条件
tetramethylsilane in tetrahydrofuran; hexane
T=-73°C; 0.0333333 h;
参考文献
Podraza, Kenneth F.; Bassfield, Ronald L.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2643 - 2644
反应条件
in tetrahydrofuran; diethyl ether
T=27°C; Equilibrium constant;
参考文献
Fraser, Robert R.; Mansour, Tarek S.; Savard, Sylvain
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3232 - 3234
反应条件
in tetrahydrofuran
T=-47°C; Equilibrium constant;
参考文献
Fraser, Robert R.; Baignee, Alison; Bresse, Monique; Hata, Kazumi
Tetrahedron Letters, 1982 , vol. 23, # 41 p. 4195 - 4198
反应条件
in tetrahydrofuran
T=30°C; Equilibrium constant;
参考文献
Ahlbrecht, Hubertus; Schneider, Gunther
Tetrahedron, 1986 , vol. 42, # 17 p. 4729 - 4742
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane
Heating;
参考文献
Hodgson, David M.; Bray, Christopher D.; Kindon, Nicholas D.; Reynolds, Nigel J.; Coote, Steven J.; Um, Joann M.; Houk
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1019 - 1028
反应条件
zirconium oxide
6 h; Heating;
参考文献
Takahashi, Kyoko; Shibagaki, Makoto; Matsushita, Hajime
Agricultural and Biological Chemistry, 1988 , vol. 52, # 3 p. 853 - 854