3-乙酰基噻唑烷-2-硫酮合成路线 （共 15 条）
反应条件
in dichloromethane T=25°C; 0.0166667 h;
参考文献
Yang, Shyh-Chyun; Wang, Huey-Min; Chen, Ling-Ching
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1995 , vol. 42, # 3 p. 585 - 588
反应条件
in dichloromethane T=25°C; 0.0166667 h;
参考文献
Yang, Shyh-Chyun; Wang, Huey-Min; Chen, Ling-Ching
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1995 , vol. 42, # 3 p. 585 - 588
反应条件
zinc in tetrahydrofuran 1) 30 deg C, 2 h, 2) reflux, 18 h;
参考文献
Kashima, Choji; Huang, Xin Cheng; Harada, Yukari; Hosomi, Akira
Journal of Organic Chemistry, 1993 , vol. 58, # 3 p. 793 - 794
反应条件
zinc in tetrahydrofuran 1) 30 deg C, 2 h, 2) 18 h, reflux;
参考文献
Kashima, Choji; Huang, Xin Cheng; Harada, Yukari; Hosomi, Akira
Journal of Organic Chemistry, 1993 , vol. 58, # 3 p. 793 - 794
反应条件
in dichloromethane T=25°C; 6 h;
参考文献
Yang, Shyh-Chyun; Wang, Huey-Min; Chen, Ling-Ching
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1995 , vol. 42, # 3 p. 585 - 588
反应条件
T=75°C; Rate constant;
参考文献
Yamada, Shinji
Angewandte Chemie, 1993 , vol. 105, # 7 p. 1128 - 1130
反应条件
in toluene T=80°C; Acylation; 18 h;
参考文献
Journal of Organic Chemistry, , vol. 61, # 17 p. 5932 - 5938
反应条件
sodium hydride in tetrahydrofuran 4 h; Ambient temperatureselective acylation also with other 3-acylthiazolidine-2-thiones; other diols and polyols as substrates;
参考文献
Yamada, Shinji
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1591 - 1592
反应条件
in dichloromethane T=25°C; 0.0166667 h;
参考文献
Yang, Shyh-Chyun; Wang, Huey-Min; Chen, Ling-Ching
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1995 , vol. 42, # 3 p. 585 - 588
反应条件
sodium hydride in tetrahydrofuran 1 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Yamada, Shinji
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1591 - 1592
