P(MeNCH2CH2)3N in dimethyl sulfoxide T=80°C; desilylation; 36 h;

boron tribromide in dichloromethane 0.166667 h; Ambient temperature;

<b>Multi-step reaction with 2 steps<br /> </b>1: 53 percent / I₂ <br />2: acetonitrile / 16 h / 20 &deg;C<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '19240532', constants.ctx, '0')">P(MeNCH₂CH₂)3N</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=80&deg;C;&nbsp;24&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '105690', constants.ctx, '0')">2,6-dimethylpyridine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=20&deg;C;&nbsp;24&nbsp;h;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 1.) n-butyllithium / 1.) ether, O deg C, 2.) 20 h, reflux<br />2: 53 percent / I₂ <br />3: acetonitrile / 16 h / 20 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: &lt;Ph₃C&gt;ClO₄ <br />2: Py / acetonitrile<br /> <br /> &nbsp;