N,N',1,2-四苯基乙烷-1,2-二亚胺合成路线 （共 33 条）
反应条件
4-toluenesulfonyl azide; lithium diisopropyl amide
1) THF, cyclohexane, -78 deg C to 15 deg C, 2) THF, -78 deg C to 20 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Katritzky, Alan R.; Gordeev, Mikhail F.; Greenhill, John V.; Steel, Peter J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 9 p. 1111 - 1118
反应条件
lithium diisopropyl amide
1) THF, cyclohexane, -78 deg C to -15 deg C, 2) THF, -78 deg C to 20 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Katritzky, Alan R.; Gordeev, Mikhail F.; Greenhill, John V.; Steel, Peter J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 9 p. 1111 - 1118
反应条件
lithium diisopropyl amide
1) THF, cyclohexane, -78 deg C to 15 deg C, 2) THF, -78 deg C to 20 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Katritzky, Alan R.; Gordeev, Mikhail F.; Greenhill, John V.; Steel, Peter J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 9 p. 1111 - 1118
反应条件
sodium hydroxide; tetrabutyl-ammonium chloride in dichloromethane
Product distribution;
参考文献
Correia, John
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3343 - 3344
反应条件
tetrabutyl-ammonium chloride in dichloromethane; water
7 h; influence of 1 M aq. NaOH; Product distribution;
参考文献
Correia, John
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3343 - 3344
反应条件
T=150°C; unter Stickstoff; nach kurzem Erhitzen;
参考文献
Julian et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1203,1208
反应条件
in benzene
Ambient temperature;
参考文献
Sheradsky, Tuvia; Itzhak, Norbert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2389 - 2394
参考文献
Strain
Journal of the American Chemical Society, 1929 , vol. 51, p. 272
参考文献
Jaunin; Sechaud
Helvetica Chimica Acta, 1954 , vol. 37, p. 2088,2090
参考文献
Alessandri
Gazzetta Chimica Italiana, 1922 , vol. 52 I, p. 194
Gazzetta Chimica Italiana, 1924 , vol. 54, p. 438
