反应条件
magnesium in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide all manipulations under dry Ar; heating soln. of Me3SiCl containing Mg turnings (90°C), adding dropwise dichlorodimesitylgermane in THF, heating (40 min), cooling, filtering, adding hexane, adding 10percent HCl; washing hexane layers (H2O), concg. (vacuum); recrystn. (hexane/ethanol);
参考文献
Ando, Wataru; Tsumuraya, Takeshi
Organometallics, 1989 , vol. 8, p. 1467 - 1472
