in neat (no solvent) byproducts: SiCl4, SiF4, SiF3Cl; equal weights of Na2SiF6 and AlCl3 are dried under vac. and mixed, temp. is raised up to 250°C and maintained there for 30 min; distn. via a reflux cooler (first trap -120, second trap -196°C), products of the first trap are detd. by PES;
参考文献
Grabandt, O.; Lange, C. A. de; Mooyman, R.; Vernooijs, P.
Chemical Physics Letters, 1991 , vol. 184, p. 221 - 228
