反应条件
in diethyl ether; toluene all manipulations under dry, O2 free N2 atm.; AlCl3 dissolved in Et2O, soln. of iso-Bu3Al in toluene added at -78°C, allowed to warm to room temp., stirred and refluxed for for 3, stirred at room temp. for 48 h h;
参考文献
Schumann, Herbert; Dechert, Sebastian; Hummert, Markus; Lange, Katharina C. H.; Schutte, Stefan; Wassermann, Birgit C.; Koehler, Katrin; Eichhorn, Jens
Zeitschrift fur Anorganische und Allgemeine Chemie, 2004 , vol. 630, # 8-9 p. 1196 - 1204
