in neat (no solvent) absence of moisture; large excess AlCl3, evacuated quartz tube, 573 K; fractional sublimation over 450 to 650 K gradient, removal of residual AlCl3 on heating in Cl2/N2 stream;
Forbes; Anderson
Journal of the American Chemical Society, 1945 , vol. 67, p. 1912
Full Text Show Details
Kharasch; Kuderna; Urry
Journal of Organic Chemistry, 1948 , vol. 13, p. 900