in neat (no solvent) absence of moisture; large excess AlCl3, evacuated quartz tube, 573 K; fractional sublimation over 450 to 650 K gradient, removal of residual AlCl3 on heating in Cl2/N2 stream;
Norris; Sturgis
Journal of the American Chemical Society, 1939 , vol. 61, p. 1413,1416
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Norris; Arthur
Journal of the American Chemical Society, 1940 , vol. 62, p. 874,876
Kurssanow; Selwin
Zhurnal Obshchei Khimii, 1939 , vol. 9, p. 2173,2176
Chem. Zentralbl., 1940 , vol. 111, # I p. 3242
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Norris; Arthur
Journal of the American Chemical Society, 1940 , vol. 62, p. 874,876
ammonium molybdate in further solvent(s) prepn. according to D. Guay et al., J. Electrochem. Soc. 136 (1989) 2272at 220°C in 1,2,4-trichlorobenzene; purified by vac. gradient sublimation at residual pressure of 1E-4 Torr;
参考文献
Basova, Tamara V.; Kiselev, Vitaly G.; Plyashkevich, Vladimir A.; Cheblakov, Pavel B.; Latteyer, Florian; Peisert, Heiko; Chasse, Thomas
Chemical Physics, 2011 , vol. 380, # 1-3 p. 40 - 47
