in neat (no solvent) absence of moisture; large excess AlCl3, evacuated quartz tube, 573 K; fractional sublimation over 450 to 650 K gradient, removal of residual AlCl3 on heating in Cl2/N2 stream;
Miller
Journal of the American Chemical Society, 1940 , vol. 62, p. 993
Full Text View citing articles Show Details
Henne; Newman
Journal of the American Chemical Society, 1938 , vol. 60, p. 1698