sodium; ammonium chloride; tert-butyl alcohol in ammonia Irradiation (UV/VIS); Sb reacted with Na (excess) in liquid NH3; t-BuOH and C6H5Cl were added (excess of both); mixture irradiated for 60 min, quenched by NH4Cl.; Product extd. with Et2O, solvent removed; recrystn. (petroleum ether); m.p.;
参考文献
Journal of Organometallic Chemistry, , vol. 270, # 2 p. 177 - 184