1,2-双(三甲基硅氧基)乙烷合成路线 （共 58 条）
反应条件
urea T=20 - 25°C; 6 h;
参考文献
Krolevets, A. A.; Antipova, V. V.; Popov, A. G.; Adamov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 10 p. 2274 - 2281,2023 - 2030
反应条件
methyl iodide in toluene T=80 - 90°C; 12 h;
参考文献
Iwata, Arihiro; Tang, Heqing; Kunai, Atsutaka; Ohshita, Joji; Yamamoto, Yasushi; Matui, Chinami
Journal of Organic Chemistry, 2002 , vol. 67, # 15 p. 5170 - 5175
反应条件
sodium saccharine T=80 - 90°C; 2 h;
参考文献
Zhang, Y. F.; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Journal of Fluorine Chemistry, 1994 , vol. 68, # 3 p. 287 - 292
反应条件
methyl iodide in toluene T=80 - 90°C; 12 h;
参考文献
Iwata, Arihiro; Tang, Heqing; Kunai, Atsutaka; Ohshita, Joji; Yamamoto, Yasushi; Matui, Chinami
Journal of Organic Chemistry, 2002 , vol. 67, # 15 p. 5170 - 5175
反应条件
T=25°C; 0.0833333 h;
参考文献
Mai, Khuong; Patil, Ghanshyam
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3545 - 3548
反应条件
methyl iodide in toluene T=80 - 90°C; 12 h; Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 15 p. 5170 - 5175
反应条件
methyl iodide in toluene T=80 - 90°C; 12 h; Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 15 p. 5170 - 5175
反应条件
methyl iodide in toluene T=80 - 90°C; 12 h; Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 67, # 15 p. 5170 - 5175
反应条件
chloro-trimethyl-silane T=-78°C; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 11 p. 2758 - 2761
反应条件
Cp*Si(1+)* B(C6F5)4(1-) in dichloromethane-d2 T=-30°C; 120 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 30 p. 6843 - 6846
