[(2,2-二甲基丙基)硫基]苯合成路线 （共 16 条）
反应条件
1: thiophenol With sodium ethanolate
2: 1-bromo-2,2-dimethylpropane With Aliquatreg; 336 in water
T=70°C; 16 h; Inert atmosphere;
参考文献
O'Mahony, Graham E.; Eccles, Kevin S.; Morrison, Robin E.; Ford, Alan; Lawrence, Simon E.; Maguire, Anita R.
Tetrahedron, 2013 , vol. 69, # 47 p. 10168 - 10184
反应条件
diphenyldisulfane in benzene
byproducts: PhSHgCl; Irradiation (UV/VIS); nitrogen atmosphere; mercurial and PhSSPh in deoxygenated solvent irradiated (275-W sunlamp, 35-40 °C, 12h);; filtration; solvent removed (vacuum); (CH3)3CCH2SPh analysed by (1)H NMR, GLC and GCMS;;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
tributylphosphine in tetrahydrofuran
T=62°C; P=7500600 Torr; 3 h; other pressures and times; var. prim. and sec. alcohols;
参考文献
Kotsuki, Hiyoshizo; Matsumoto, Kazuhiko; Nishizawa, Hitoshi
Tetrahedron Letters, 1991 , vol. 32, # 33 p. 4155 - 4158
反应条件
in benzene
T=35 - 40°C; 12 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
1: TsOH / xylene / 140 °C
View Scheme
参考文献
Vedejs, E.; Perry, D. A.
Journal of the American Chemical Society, 1983 , vol. 105, # 6 p. 1683 - 1684
反应条件
in benzene
T=45°C; 12 h; Irradiation;
参考文献
Russell, Glen A.; Tashtoush, Hasan
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1398 - 1399
反应条件
in chloroform-d1
T=20°C; 8 h;
参考文献
Hao, Wei; Fujii, Takayoshi; Dong, Tiaoling; Wakai, Youko; Yoshimura, Toshiaki
Heteroatom Chemistry, 2004 , vol. 15, # 3 p. 193 - 198
反应条件
potassium tert-butylate in dimethyl sulfoxide
1 h; Inert atmosphereIrradiation;
参考文献
Barrionuevo, Cecilia A.; Argueello, Juan E.; Penenory, Alicia B.
Arkivoc, 2011 , vol. 2011, # 7 p. 245 - 259
反应条件
in diethyl ether; cyclohexane
0 deg C, 0.5 h then warming to 20 deg C, 0.5 h;
参考文献
Vedejs, Edwin; Perry, David A.; Wilde, Richard G.
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 2985 - 2989
反应条件
in ammonia
T=-33°C; 90 h; Irradiationother nucleophiles, other time, other reagents; Product distributionMechanism;
参考文献
Pierini, Adriana B.; Penenory, Alicia B.; Rossi, Roberto A.
Journal of Organic Chemistry, 1985 , vol. 50, # 15 p. 2739 - 2742
