in methanol byproducts: N2, HCl; addn. of the isocyanide to the Re compd. in MeOH and refluxing for 2 h; concn. (vac.), addn. of Et2O and petroleum ether and recrystn. from CH2Cl2-Et2O;
参考文献
Carvalho, M. Fernanda N. N.; Pombeiro, Armando J. L.
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 121 - 132
Klages; Moenkemeyer
Chemische Berichte, 1952 , vol. 85, p. 126
→
反应条件
in tetrahydrofuran byproducts: N2; addn. of the isocyanide to the Re compd. in THF and stirring for 2 h at room temp.; filtn., concn. (vac.), addn. of CH2Cl2 or THF, then Et2O, filtn., washing with Et2O and drying in vac.;
参考文献
Carvalho, M. Fernanda N. N.; Pombeiro, Armando J. L.
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 121 - 132
in methanol byproducts: N2, HCl; addn. of the isocyanide to the Re compd. in MeOH and refluxing for 2 h; concn. (vac.), addn. of Et2O and petroleum ether and recrystn. from CH2Cl2-Et2O;
参考文献
Carvalho, M. Fernanda N. N.; Pombeiro, Armando J. L.
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 121 - 132
