2,4-二甲氧基-3-甲基苯甲醛合成路线 （共 22 条）
反应条件
titanium tetrachloride in dichloromethane T=0 - 20°C; 2 h;
参考文献
Yoshida, Atsushi; Asakawa, Tomohiro; Hamashima, Yoshitaka; Kan, Toshiyuki; Akaiwa, Michinori; Yokoshima, Satoshi; Fukuyama, Tohru
Chemistry--A European Journal, 2012 , vol. 18, # 36 p. 11192 - 11195,4
反应条件
trichlorophosphate T=60°C;
参考文献
Wu, Yan-Chao; Zhu, Jieping
Organic Letters, 2009 , vol. 11, # 23 p. 5558 - 5561
反应条件
1: 2,6-dimethoxytoluene With tin(IV) chloride in dichloromethane T=0°C; 1 h; 2: chloromethyl methyl ether in dichloromethane T=0 - 25°C;
参考文献
Coleman, Robert S.; Felpin, Francois-Xavier; Chen, Wei
Journal of Organic Chemistry, 2004 , vol. 69, # 21 p. 7309 - 7316
参考文献
Abbott Laboratories
Patent: US4456612 A1, 1984 ;
反应条件
potassium carbonate in acetone 5 h; Heating;
参考文献
Barber, Jill; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1685 - 1689
反应条件
1: phenyl lithium; diethyl ether / Erwaermen der Reaktionsloesung mit Dimethylsulfat 2: POCl3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 78, p. 771,773
参考文献
Journal of the American Chemical Society, , vol. 78, p. 771,773
反应条件
1: HCl 2: K2CO3 / acetone / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 49 p. 8829 - 8832
反应条件
Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 49, # 6 p. 1078 - 1083
反应条件
1: MCPBA / CH2Cl2 / 5 h / 20 °C 2: aq. NaOH / methanol / 4 h / 20 °C 3: aq. CAN / acetonitrile / 1 h / 20 °C View Scheme
参考文献
Heckrodt, Thilo J.; Mulzer, Johann
Journal of the American Chemical Society, 2003 , vol. 125, # 16 p. 4680 - 4681
