1: With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=-40°C; 2: With hydrogenchloride in tetrahydrofuran Further stages. Title compound not separated from byproducts.;
tert-butylhypochlorite; Na(1+) faujasite X; hydrogen cation in acetonitrile T=40°C; 336 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;