磷酸二叔丁基酯四正丁基铵盐合成路线 （共 8 条）
反应条件
tetra(n-butyl)ammonium hydroxide in methanol T=26°C; pH=6.5 - 7.0; 0.7 h;
参考文献
EISAI CO., LTD.
Patent: WO2006/118351 A1, 2006 ;
Location in patent: Page/Page column 56-58 ;
反应条件
in water; acetone Cooling with ice;
参考文献
MERCK PATENT GESELLSCHAFT MIT BESCHRANKTER HAFTUNG; Eggenweiler, Hans-Michael; Sirrenberg, Christian; Buchstaller, Hans-Peter
Patent: US2013/178443 A1, 2013 ;
Location in patent: Paragraph 0934; 0935 ;
反应条件
1: potassium permanganate; potassium hydrogencarbonate / water / 1.42 h / 0 - 60 °C 2: water; acetone / |Cooling with ice View Scheme
反应条件
(i) aq. NaOH, (ii) /BRN= 4165042/; Multistep reaction;
参考文献
Synthesis, , p. 770 - 771
反应条件
in benzene T=20°C; 3 h;
参考文献
WO2006/118351 A1, ;
Page/Page column 56-58 ;
反应条件
in ethylene glycol dimethyl ether
Heating;
参考文献
Kluba,M.; Zwierzak,A.
Synthesis, 1978 , p. 770 - 771
反应条件
in ethylene glycol dimethyl ether
Heating;
参考文献
Kluba,M.; Zwierzak,A.
Synthesis, 1978 , p. 770 - 771
反应条件
in ethylene glycol dimethyl ether
Heating;
参考文献
Kluba,M.; Zwierzak,A.
Synthesis, 1978 , p. 770 - 771
