(4-溴苯氧基)叔丁基二甲基硅烷合成路线 （共 45 条）
反应条件
1H-imidazole in N,N-dimethyl-formamide T=35°C; 0.5 h;
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 3144 - 3177
反应条件
1: With 1H-imidazole in DMF (N,N-dimethyl-formamide) T=40°C; 2 h; 2: With N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 0.5 h; Sun lampHeating / reflux;
参考文献
US6706839 B1, ;
Page column 15 ;
反应条件
scandium tris(trifluoromethanesulfonate) in various solvent(s) T=20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 41, # 46 p. 8903 - 8906
反应条件
18-crown-6 ether; potassium carbonate T=150°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 27, # 41 p. 4995 - 4998
反应条件
in water; N,N-dimethyl-formamide
反应条件
hydrogenchloride; N-bromosuccinmide in acetone T=20°C; Bromination; 0.0166667 h;
参考文献
Synthetic Communications, , vol. 30, # 12 p. 2091 - 2098
反应条件
2: 94 percent / Sc(OTf)3 / various solvent(s) / 2 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 46 p. 8903 - 8906
反应条件
sodium methylate 1.) DMF, rt, 30 min, 2.) DMF, rt, 1 h; Yield givenMultistep reaction;
参考文献
Synthetic Communications, , vol. 29, # 13 p. 2217 - 2223
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C 1.2: triisopropyl borate / tetrahydrofuran; hexane / -78 - 0 °C 1.3: 97 percent / HCl / tetrahydrofuran; hexane; H2O 2.1: 128 mg / Na2CO3 / Pd(PPH3)4 / toluene; H2O / 2 h / 85 °C 3.1: tetrabutylammonium fluoride / tetrahydrofuran / 0.08 h View Scheme
参考文献
Hajduk; Sheppard; Nettesheim; Olejniczak; Shuker; Meadows; Steinman; Carrera Jr.; Marcotte; Severin; Walter; Smith; Gubbins; Simmer; Holzman; Morgan; Davidsen; Summers; Fesik
Journal of the American Chemical Society, 1997 , vol. 119, # 25 p. 5818 - 5827
