反式-BETA-苯乙烯硼酸合成路线 （共 109 条）
反应条件
in tetrahydrofuran T=23°C; 3 h;
参考文献
Yoo, Kyung Soo; Yoon, Cheol Hwan; Jung, Kyung Woon
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16384 - 16393
参考文献
University of Southern California
Patent: US6232467 B1, 2001 ;
反应条件
multistep reaction; other substrates, other boronic acids; E-selectivity; Mechanism;
参考文献
Tetrahedron Letters, , vol. 34, # 4 p. 583 - 586
反应条件
Najera palladacycle I; tetra(n-butyl)ammonium hydroxide; potassium carbonate; [HP(t-Bu)3]BF4 in N,N-dimethyl-formamide T=130°C; Suzuki-Miyaura alkenylation; 0.333333 h; Microwave irradiation; regioselective reaction;
参考文献
Civicos, Jose F.; Alonso, Diego A.; Najera, Carmen
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1683 - 1687
反应条件
1: MgSO4 / diethyl ether / 9 h / 20 °C 2: 85 percent / 1-phenylpropyne; H2O / Ni(cod)2 / dioxane / 12 h / 80 °C View Scheme
参考文献
Takahashi, Go; Shirakawa, Eiji; Tsuchimoto, Teruhisa; Kawakami, Yusuke
Chemical Communications, 2005 , # 11 p. 1459 - 1461
反应条件
dipotassium peroxodisulfate; Bi(NO3)3·5H2O in benzene T=70°C; 12 h; Inert atmosphere;
参考文献
Manna, Srimanta; Maity, Soham; Rana, Sujoy; Agasti, Soumitra; Maiti, Debabrata
Organic Letters, 2012 , vol. 14, # 7 p. 1736 - 1739
反应条件
magnesium sulfate in diethyl ether T=20°C; 9 h;
参考文献
Oda, Susumu; Yamamoto, Hisashi
Angewandte Chemie - International Edition, 2013 , vol. 52, # 31 p. 8165 - 8168
Angew. Chem., 2013 , vol. 125, # 31 p. 8323 - 8326,4
反应条件
sodium iodide in N,N-dimethyl-formamide 16 h; Ambient temperature;
参考文献
Murata, Miki; Satoh, Kaname; Watanabe, Shinji; Masuda, Yuzuru
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 9 p. 1465 - 1466
反应条件
1.1: 92 percent / KHF2 / methanol; H2O / 20 °C 2.1: HBF4; NaNO2 / H2O / 0.5 h / 0 - 5 °C 2.2: 96 percent / Pd2(μ-OAc)2(P(o-tolyl)3)2 / methanol / 0.02 h / 20 °C View Scheme
参考文献
Darses, Sylvain; Michaud, Guillaume; Genet, Jean-Pierre
European Journal of Organic Chemistry, 1999 , # 8 p. 1875 - 1883
反应条件
Najera palladacycle I; tetra(n-butyl)ammonium hydroxide; potassium carbonate; [HP(t-Bu)3]BF4 in N,N-dimethyl-formamide T=130°C; Suzuki-Miyaura alkenylation; 0.333333 h; Microwave irradiation; regioselective reaction;
参考文献
Civicos, Jose F.; Alonso, Diego A.; Najera, Carmen
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1683 - 1687
