[(叔丁基二甲基甲硅烷基)氧基]乙酸乙酯合成路线 （共 6 条）
反应条件
1H-imidazole in N,N-dimethyl-formamide 1 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 67, # 6 p. 1708 - 1716
反应条件
1: 1H-imidazole / dimethylformamide 2: (i) (COCl)2, DMF, CH2Cl2, (ii) /BRN= 1718733/, Py View Scheme
参考文献
Journal of Organic Chemistry, , vol. 43, p. 3972 - 3974
反应条件
(i) (COCl)2, DMF, CH2Cl2, (ii) /BRN= 1718733/, Py; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 43, p. 3972 - 3974
反应条件
1: With potassium hydroxide in ethanol T=0 - 20°C; Inert atmosphere; 2: With hydrogenchloride in water pH=3 - 4; Inert atmosphere;
参考文献
Liu, Lian Jin; Yoo, Jin Cheol; Hong, Joon Hee
Nucleosides, Nucleotides and Nucleic Acids, 2008 , vol. 27, # 10-11 p. 1186 - 1196
反应条件
diisobutylaluminium hydride in diethyl ether; hexane T=-78°C;
参考文献
Roos, Juergen; Effenberger, Franz
Tetrahedron Asymmetry, 1999 , vol. 10, # 14 p. 2817 - 2828
反应条件
1.1: potassium hydroxide / ethanol / 12 h / 0 - 23 °C / Inert atmosphere
1.2: 0 °C / pH 4 / Inert atmosphere
2.1: oxalyl dichloride / benzene / 1 h / 23 - 90 °C / Inert atmosphere
View Scheme
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
