3,4-双(甲氧基甲氧基)苯甲醛合成路线 （共 15 条）
反应条件
4-(N,N-dimethlyamino)pyridine; N-ethyl-N,N-diisopropylamine in dichloromethane
T=0°C; Inert atmosphereReflux;
参考文献
Saiz-Poseu, Javier; Faraudo, Jordi; Figueras, Antoni; Alibes, Ramon; Busque, Felix; Ruiz-Molina, Daniel
Chemistry - A European Journal, 2012 , vol. 18, # 10 p. 3056 - 3063
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran
T=20°C; Cooling with ice;
参考文献
Fumeaux, Rene; Menozzi-Smarrito, Candice; Stalmach, Angelique; Munari, Caroline; Kraehenbuehl, Karin; Steiling, Heike; Crozier, Alan; Williamson, Gary; Barron, Denis
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 22 p. 5199 - 5211
反应条件
toluene-4-sulfonic acid in dichloromethane
参考文献
Yardley,J.P. et al.
Synthesis, 1976 , p. 244
反应条件
1: 1.55 g / KOH / ethanol / 72 h / 20 °C
2: 0.345 g / aq. HCl / methanol / 0.25 h / Heating
3: DDQ / dioxane / 3 h / Heating
View Scheme
参考文献
Hossain, M. Amzad; Ismail, Zhari
Pakistan Journal of Scientific and Industrial Research, 2004 , vol. 47, # 4 p. 268 - 271
反应条件
sodium tetrahydroborate in ethanol
T=20°C;
参考文献
Wang, Yanming; Mathis, Chester A.; Huang, Guo-Feng; Holt, Daniel P.; Debnath, Manik L.; Klunk, William E.
Journal of Labelled Compounds and Radiopharmaceuticals, 2002 , vol. 45, # 8 p. 647 - 664
