4-甲基-7H-苯并[de]蒽-7-酮合成路线 （共 17 条）
反应条件
sodium dichromate in acetic acid
Heating;
参考文献
Prostakov, N. S.; Pleshakov, V. G.; Zainul Abedin, Md.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2199 - 2200
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2462 - 2463
反应条件
1: 7 percent / K-16 / 550 - 580 °C
2: 43 percent / sodium bichromate / acetic acid / Heating
View Scheme
参考文献
Prostakov, N. S.; Pleshakov, V. G.; Zainul Abedin, Md.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2199 - 2200
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2462 - 2463
反应条件
1: acetic anhydride / Heating
2: 7 percent / K-16 / 550 - 580 °C
3: 43 percent / sodium bichromate / acetic acid / Heating
View Scheme
参考文献
Prostakov, N. S.; Pleshakov, V. G.; Zainul Abedin, Md.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2199 - 2200
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2462 - 2463
反应条件
1: acetic anhydride / Heating
2: 7 percent / K-16 / 550 - 580 °C
3: 43 percent / sodium bichromate / acetic acid / Heating
View Scheme
参考文献
Prostakov, N. S.; Pleshakov, V. G.; Zainul Abedin, Md.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2199 - 2200
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2462 - 2463
反应条件
1: acetic anhydride / Heating
2: 7 percent / K-16 / 550 - 580 °C
3: 43 percent / sodium bichromate / acetic acid / Heating
View Scheme
参考文献
Prostakov, N. S.; Pleshakov, V. G.; Zainul Abedin, Md.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2199 - 2200
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2462 - 2463
反应条件
aluminium trichloride
Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit wss. Schwefelsaeure und Glycerin auf 125-130grad;
参考文献
Steyermark; Gardner
Journal of the American Chemical Society, 1930 , vol. 52, p. 4884,4886
反应条件
aluminium trichloride
T=150°C;
参考文献
Mayer; Sieglitz
Chemische Berichte, 1922 , vol. 55, p. 1840,2940
Full Text Show Details
Mayer; Fleckenstein; Guenther
Chemische Berichte, 1930 , vol. 63, p. 1464,1469
反应条件
sulfuric acid; copper(II) sulfate; glycerol
T=120 - 130°C; weiteres Reagens: Zink-Pulver;
参考文献
Newport Chem. Corp.
Patent: US1791309 , 1928 ;
反应条件
sulfuric acid
T=110°C; Behandeln des mit Wasser versetzten Reaktionsgemisches mit Glycerin und Eisen-Pulver bei 112-118grad;
参考文献
du Pont de Nemours and Co.
Patent: US2034485 , 1933 ;
反应条件
sulfuric acid; glycerol
T=100 - 120°C;
参考文献
Mayer; Fleckenstein; Guenther
Chemische Berichte, 1930 , vol. 63, p. 1464,1469
