1: 2-methyl propane; carbon monoxide With hydrogen fluoride; SbF5 T=0°C; Carbonylation; 1 h; 2: ethanol With bicarbonate T=-78°C; Esterification; Further byproducts given. Title compound not separated from byproducts;
参考文献
Sommer, Jean; Bukala, Jozef; Hachoumy, Mohammed; Jost, Roland
Journal of the American Chemical Society, 1997 , vol. 119, # 14 p. 3274 - 3279
toluene-4-sulfonic acid; bis-triphenylphosphine-palladium(II) chloride in various solvent(s) T=119.85°C; P=45003.6 Torr; 12 h; in ionic liquid; Product distribution; Further Variations:CatalystsSolventsTemperatures;
参考文献
Qiao, Kun; Deng, Youquan
New Journal of Chemistry, 2002 , vol. 26, # 5 p. 667 - 670