2,5-环己二烯-1,4-二酮单肟合成路线 （共 96 条）
参考文献
Geigy and Co.
Patent: DE71368 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 57
反应条件
1: 45 percent / HCl (gas) / diethyl ether / 1 h / -10 - 0 °C
2: 82 percent / K2CO3; CuI; Cu / toluene / 48 h / Heating
3: 81 percent / BBr3 / CH2Cl2; 1,2-dichloro-ethane / 1 h / 20 °C
View Scheme
参考文献
Kim, Sang-Hyun; Kwon, Jung-Hwan; Yoon, Sung-Hwa
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 10 p. 3007 - 3009
参考文献
Dostal
Acta Univ. Palacki. Olomuc. Fac. rerum nat., 1977 , vol. 53, p. 85,86
参考文献
Hays,J.T. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 153 - 158
反应条件
ethanol; water
T=20°C;
参考文献
Borsche
Justus Liebigs Annalen der Chemie, 1905 , vol. 343, p. 190
反应条件
hydrogenchloride in 1,4-dioxane
T=20°C; 1 h; Inert atmosphere;
参考文献
Kim, Sang-Hyun; Kwon, Jung-Hwan; Yoon, Sung-Hwa
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 10 p. 3007 - 3009
参考文献
Jaeger
Chemische Berichte, 1875 , vol. 8, p. 897
Full Text Show Details
Bargellini; Leone
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1928 , vol. <6>8, p. 399
Chem. Zentralbl., 1929 , vol. 100, # I p. 1441
反应条件
2: NH4SH
View Scheme
参考文献
Petersen et al.
Angewandte Chemie, 1955 , vol. 67, p. 217,219
反应条件
i-AmNO2; potassium carbonate in N,N-dimethyl-formamide
24 h; Ambient temperature;
参考文献
Ishikawa, Tsutomu; Watanabe, Toshiko; Tanigawa, Hisashi; Saito, Tatsuru; Kotake, Ken-Ichiro; Ohashi, Yoshiaki; Ishii, Hisashi
Journal of Organic Chemistry, 1996 , vol. 61, # 8 p. 2774 - 2779
反应条件
phosphoric acid; μ-superoxobis[pentaaminecobalt(III)](ClO4)5 in water
T=25°C; KineticsMechanism; SolventTemperature;
参考文献
Singh, Bula; Das, Ranendu Sekhar; Banerjee, Rupendranath; Mukhopadhyay, Subrata
Inorganica Chimica Acta, 2013 , vol. 406, p. 266 - 271
