Erhitzen des vom Loesungsmittel befreiten Reaktionsgemisches auf 135-140grad;
参考文献
Edkins; Linnell
Quarterly Journal of Pharmacy and Pharmacology, 1936 , vol. 9, p. 203,215
Full Text Show Details
Hartung et al.
Journal of the American Chemical Society, 1931 , vol. 53, p. 4149,4154
in toluene byproducts: H2; EtCO2Ph added to CoH(N2)(PPh3)3 in toluene in vac., reacted for 3 days at room temp.; liquid phase analysed by GLC; hexane added, ppt. filtered, washed with hexane, dried in vac., recrystd. from C6H6-hexane;
参考文献
Journal of the American Chemical Society, , vol. 108, # 3 p. 385 - 391
in toluene AcOPh added to CoMe(PPh3)3, evacuated, stirred at 0°C for 5 h, gradually warmed to room temp., reacted for 1 day; hexane added, ppt. filtered, washed with hexane, dried in vac.;
参考文献
Journal of the American Chemical Society, , vol. 108, # 3 p. 385 - 391
