2-(4-氯苯基)-1-苯乙酮合成路线 (共 67 条)
反应条件
bis(acetylacetonate)nickel(II) in tetrahydrofuran T=20°C; Negishi coupling reaction; 0.166667 h;
参考文献
Kim, Seung-Hoi; Rieke, Reuben D.
Tetrahedron Letters, 2011 , vol. 52, # 13 p. 1523 - 1526
反应条件
AlCl3, aluminium chloride in dichloromethane T=0 - 20°C; Friedel-Crafts Acylation; 0.5 h; Inert atmosphere;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Iazzetti, Antonia; Verdiglione, Rosanna
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-Z0055-OP, p. 1701 - 1707
反应条件
nickel in ethylene glycol dimethyl ether T=85°C; 0.25 h;
参考文献
Inaba, Shin-ichi; Rieke, Reuben D.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2451 - 2452
Title/Abstract Full Text View citing articles Show Details
Inaba, Shin-ichi; Rieke, Reuben D.
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1373 - 1381
反应条件
[NiCl2(1,2-dimethoxyethane)]; 1,3-bis-(diphenylphosphino)propane; water; zinc in ethylene glycol dimethyl ether T=100°C; 36 h;
参考文献
Hsieh, Jen-Chieh; Chen, Yen-Chung; Cheng, An-Yi; Tseng, Hsiao-Chun
Organic Letters, 2012 , vol. 14, # 5 p. 1282 - 1285
反应条件
tri-ruthenium(0)dodecacarbonyl in toluene T=120°C; 40 h;
参考文献
Tatamidani, Hiroto; Yokota, Kazuhiko; Kakiuchi, Fumitoshi; Chatani, Naoto
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5615 - 5621
反应条件
lithium diisopropyl amide in tetrahydrofuran T=0°C; 4 h; adding, -70 deg C;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2496 - 2502
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in tetrahydrofuran T=80°C; 3 h; Schlenk tubeInert atmosphere;
参考文献
Rao, Maddali L.N.; Giri, Somnath; Jadhav, Deepak N.
Tetrahedron Letters, 2009 , vol. 50, # 45 p. 6133 - 6138
反应条件
palladium(II) dichloride bis[bis(diphenylphosphine)ferrocene] dichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide T=100°C; Stille coupling; 16 h;
参考文献
Saevmarker, Jonas; Lindh, Jonas; Nilsson, Peter
Tetrahedron Letters, 2010 , vol. 51, # 52 p. 6886 - 6889
反应条件
tris(trifluoroacetoxy)-λ3-iodane in tetrachloromethane T=23°C; 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 10 p. 3182 - 3186
反应条件
1: diethyl 4-chlorobenzyl phosphate With manganese in tetrahydrofuran T=20°C; 8 h; 2: benzoyl chloride in tetrahydrofuran T=20°C; 1 h;
参考文献
Suh, YoungSung; Lee, Jun-Sik; Kim, Seoung-Hoi; Rieke, Reuben D.
Journal of Organometallic Chemistry, 2003 , vol. 684, # 1-2 p. 20 - 36