7-(氯甲基)苯并[a]蒽合成路线 (共 17 条)
反应条件
1: 88 percent / dimethylsulfoxide / 2 h / 70 °C 2: 85 percent / KOH / ethane-1,2-diol; H2O / 24 h / Heating View Scheme
参考文献
Sangaiah, R.; Gold, A.; Toney, G. E.
Journal of Organic Chemistry, 1983 , vol. 48, # 10 p. 1632 - 1638
反应条件
1: glacial acetic acid 2: ethanolic NaOH View Scheme
参考文献
Badger; Cook
Journal of the Chemical Society, 1939 , p. 802,805
参考文献
Badger; Cook
Journal of the Chemical Society, 1939 , p. 802,805
反应条件
1: 88 percent / dimethylsulfoxide / 2 h / 70 °C 2: 85 percent / KOH / ethane-1,2-diol; H2O / 24 h / Heating 3: anhydrous HF / 24 h / Ambient temperature 4: NaBH4 / tetrahydrofuran; methanol 5: Al2O3 / benzene / 0.75 h / Heating View Scheme
参考文献
Sangaiah, R.; Gold, A.; Toney, G. E.
Journal of Organic Chemistry, 1983 , vol. 48, # 10 p. 1632 - 1638
反应条件
1: 88 percent / dimethylsulfoxide / 2 h / 70 °C 2: 85 percent / KOH / ethane-1,2-diol; H2O / 24 h / Heating 3: anhydrous HF / 24 h / Ambient temperature 4: NaBH4 / tetrahydrofuran; methanol 5: Al2O3 / benzene / 0.75 h / Heating View Scheme
参考文献
Sangaiah, R.; Gold, A.; Toney, G. E.
Journal of Organic Chemistry, 1983 , vol. 48, # 10 p. 1632 - 1638
反应条件
1,4-dioxane; hydrogenchloride; tin(ll) chloride Erwaermen auf dem Dampfbad;
参考文献
Wood; Fieser
Journal of the American Chemical Society, 1940 , vol. 62, p. 2674,2678
参考文献
Wood; Fieser
Journal of the American Chemical Society, 1940 , vol. 62, p. 2674,2678
参考文献
Badger; Cook
Journal of the Chemical Society, 1939 , p. 802,805
反应条件
hydrogenchloride; acetic acid
T=60°C;
参考文献
Badger; Cook
Journal of the Chemical Society, 1939 , p. 802,805
反应条件
hydrogenchloride; acetic acid
T=60°C;
参考文献
Badger; Cook
Journal of the Chemical Society, 1939 , p. 802,805