N,N-二乙基癸烷-1-胺合成路线 （共 7 条）
反应条件
palladium 10 on activated carbon; ammonium acetate; hydrogen
T=20°C; P=760.051 Torr; 27 h;
参考文献
Ikawa, Takashi; Fujita, Yuki; Mizusaki, Tomoteru; Betsuin, Sae; Takamatsu, Haruki; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 2 p. 293 - 304
反应条件
hydrogen; copper
T=240°C; P=7600 Torr;
参考文献
Kozlov; Tereshko; Basalaeva; Tarasevich
Russian Journal of General Chemistry, 1998 , vol. 68, # 7 p. 1095 - 1098
反应条件
in ethanol
24 h; Reflux;
参考文献
Zhang, Qi; Gao, Zhinong; Xu, Feng; Tai, Shuxin; Liu, Xueguo; Mo, Shaobo; Niu, Fei
Langmuir, 2012 , vol. 28, # 33 p. 11979 - 11987
反应条件
sodium tetrahydroborate; titanium tetrachloride in ethylene glycol dimethyl ether
14 h; Ambient temperature;
参考文献
Kano, Shinzo; Tanaka, Yasuyuki; Sugino, Eiichi; Hibino, Sstoshi
Synthesis, 1980 , # 9 p. 695 - 697
反应条件
palladium 10 on activated carbon; hydrogen in methanol
T=20°C; P=760.051 Torr; 48 h;
参考文献
Ikawa, Takashi; Fujita, Yuki; Mizusaki, Tomoteru; Betsuin, Sae; Takamatsu, Haruki; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 2 p. 293 - 304
反应条件
sodium (tert-butylamino)trihydroborate in tetrahydrofuran
T=66°C; 96 h; further reducing agent: sodium (dimethylamino)trihydroborat (NaDMAB); Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hutchins, Robert O.; Learn, Keith; El-Telbany, Farag; Stercho, Yuriy P.
Journal of Organic Chemistry, 1984 , vol. 49, # 13 p. 2438 - 2443
反应条件
[rhodium(I)(carbonyl)2(acetylacetonate)]; tri-ruthenium(0)dodecacarbonyl; water; triphenylphosphine in N,N-dimethyl-formamide
T=170°C; 6 h; AutoclaveGreen chemistry; Temperature;
参考文献
Karakhanov, Eduard; Maksimov, Anton; Kardasheva, Yulia; Runova, Elena; Zakharov, Roman; Terenina, Maria; Kenneally, Corey; Arredondo, Victor
Catalysis Science and Technology, 2014 , vol. 4, # 2 p. 540 - 547
