反应条件
1: 26 percent / sodium hydride / 1,2-dimethoxy-ethane; dimethylformamide / 1.58 h / Ambient temperature 2: 1.) LiAlH4 2.) pyridin / 1.) ether, 0 deg C, 30 min 2.) 14 h, room temperature 3: 1.) RuO2, NaIO4 2.) HCl / 1.) aceton, water, 48 h, room temperature 2.) 2.5 d, room temperature View Scheme
参考文献
Schubert, Thomas; Kunisch, Franz; Welzel, Peter
Tetrahedron, 1983 , vol. 39, # 13 p. 2211 - 2217
