3,8-双-(乙氧基羰氨基)-6-苯菲啶合成路线 （共 14 条）
反应条件
1: N,N-dimethyl-acetamide / 0.5 h 2: 59 percent / diluted H2SO4 / 0.33 h / 150 °C View Scheme
参考文献
Lion, C.; Boukou-Poba, J. P.; Charvy, C.
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 3 p. 171 - 181
反应条件
nitrobenzene Erhitzen des Reaktionsprodukts mit wss. H2SO4 und anschliessendes Behandeln mit wss. NH3 und NH4Br;
参考文献
Watkins
Journal of the Chemical Society, <1952> 3059, 3062
反应条件
pyridine
T=20°C; 5 h;
参考文献
Rangarajan, Subhashree; Friedman, Simon H.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 8 p. 2267 - 2273
反应条件
trichlorophosphate
0.75 h; Heating;
参考文献
Lion, C.; Boukou-Poba, J. P.; Charvy, C.
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 3 p. 171 - 181
反应条件
1: iron-powder; aq.-ethanolic HCl
2: pyridine
View Scheme
参考文献
Watkins
Journal of the Chemical Society, <1952> 3059, 3061
反应条件
1: 92 percent / N,N-diethylaniline / ethanol / 0.17 h / Heating
2: 93 percent / iron, hydrochlorid acid / Heating; 1) water, 1 h, 2) aqueous ethanol, 20 min
3: 77 percent / nitrobenzene / Heating
4: 66 percent / POCl3 / 0.75 h / Heating
View Scheme
参考文献
Lion, C.; Boukou-Poba, J. P.; Charvy, C.
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 3 p. 171 - 181
反应条件
1: 77 percent / nitrobenzene / Heating
2: 66 percent / POCl3 / 0.75 h / Heating
View Scheme
参考文献
Lion, C.; Boukou-Poba, J. P.; Charvy, C.
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 3 p. 171 - 181
反应条件
1: 93 percent / iron, hydrochlorid acid / Heating; 1) water, 1 h, 2) aqueous ethanol, 20 min
2: 77 percent / nitrobenzene / Heating
3: 66 percent / POCl3 / 0.75 h / Heating
View Scheme
参考文献
Lion, C.; Boukou-Poba, J. P.; Charvy, C.
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 3 p. 171 - 181
反应条件
1: 93 percent / 100percent sulfuric acid, potassium nitrate / 1 h / 15 - 20 °C
2: 92 percent / N,N-diethylaniline / ethanol / 0.17 h / Heating
3: 93 percent / iron, hydrochlorid acid / Heating; 1) water, 1 h, 2) aqueous ethanol, 20 min
4: 77 percent / nitrobenzene / Heating
5: 66 percent / POCl3 / 0.75 h / Heating
View Scheme
参考文献
Lion, C.; Boukou-Poba, J. P.; Charvy, C.
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 3 p. 171 - 181
反应条件
1: nitric acid / tetrachloromethane
2: hydrogen / ethanol / 60 °C / 22052.2 Torr
3: sulfuric acid; potassium nitrate
4: tin(IV) chloride / nitrobenzene
5: NH2NH2•xH2O / ethanol / 1 h / 75 °C
6: pyridine
View Scheme
参考文献
Osadchii; Shubin; Kozlova; Varlamenko; Filipenko; Boyarskikh
Russian Journal of Applied Chemistry, 2011 , vol. 84, # 9 p. 1541 - 1548
