反-1,3-二苯基-2-丙稀-1-醇合成路线 (共 76 条)
反应条件
in tetrahydrofuran Addition;
参考文献
Journal of Organic Chemistry, , vol. 63, # 17 p. 5730 - 5731
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran T=-60°C; 2: With dihydrogen peroxide in tetrahydrofuran; water T=0 - 20°C; 1.33333 h;
参考文献
Tetrahedron Letters, , vol. 43, # 31 p. 5495 - 5497
反应条件
sodium hydride; (R)-1,1'-bis(diphenylphosphino)-2,2'-binapthyl; palladium/alumina in tetrahydrofuran T=120°C; 3 h; Title compound not separated from byproducts.;
参考文献
Journal of Catalysis, , vol. 252, # 1 p. 30 - 38
反应条件
1: With [RuN(saldach)(CH3OH)](+)[ClO4](-); phenyl silane in toluene 20 h; Reflux; 2: With hydrogenchloride in diethyl ether; water; toluene
参考文献
ACS Catalysis, , vol. 3, # 4 p. 678 - 684
反应条件
triethylammonium phosphinate; tris(triphenylphosphine)ruthenium(II) chloride T=40°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 37, # 36 p. 6599 - 6602
参考文献
European Journal of Organic Chemistry, , # 1 p. 99 - 104
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane T=-100°C; 1 h; Further byproducts given;
参考文献
Tetrahedron, , vol. 59, # 11 p. 1995 - 2000
反应条件
1: 2,4-dimethyl-3-pentyl α-trimethylsilanylacetate With lithium diisopropyl amide in tetrahydrofuran 2: trans-1,3-diphenyl-2-propen-1-one in tetrahydrofuran T=-78°C;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 52, # 1 p. 125 - 129
反应条件
ATPH in hexane; toluene T=-78°C; 0.25 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 38, # 22 p. 3951 - 3954
反应条件
1: bis(2-phenylethenyl)telluride With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Metallation; 0.333333 h; 2: benzaldehyde in tetrahydrofuran; hexane T=-78°C; Addition; 0.5 h; Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 584, # 1 p. 44 - 47