反应条件
1: sulfuric acid / 120 - 125 °C
2: potassium carbonate / acetone / 3 h / |Reflux
3: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 25 - 35 °C
4: N-ethyl-N,N-diisopropylamine / dichloromethane / 25 - 35 °C
5: acetonitrile / 12 h / 35 - 40 °C
6: hydrogen / methanol / 25 - 30 °C / 2625.26 Torr / |Autoclave
View Scheme
参考文献
Srinivas, Keesari; Srinivasan, Neti; Reddy, Kikkuru Srirami; Ramakrishna, Muddasani; Reddy, Chinta Raveendra; Arunagiri, Muthulingam; Kumari, Routhu Lalitha; Venkataraman, Sundaram; Mathad, Vijayavitthal T.
Organic Process Research and Development, 2005 , vol. 9, # 3 p. 314 - 318