4,4’-二甲基二苯硫醚合成路线 （共 108 条）
反应条件
[2,2']bipyridinyl; copper(l) iodide; sulfur; aluminium; magnesium chloride in N,N-dimethyl-formamide
T=110°C; 43 h;
参考文献
Taniguchi, Nobukazu
Synlett, 2005 , # 11 art. no. U10105ST, p. 1687 - 1690
反应条件
C25H29Cl2N2PPd; potassium tert-butylate in toluene
T=20°C; 8.16667 h; Inert atmosphereReflux;
参考文献
Fu, Ching-Feng; Liu, Yi-Hung; Peng, Shei-Ming; Liu, Shiuh-Tzung
Tetrahedron, 2010 , vol. 66, # 12 p. 2119 - 2122
反应条件
toluene-4-sulfonic acid; potassium iodide in solid
T=30°C; 30 h;
参考文献
Fujiki, Kiyoko; Kurita, Shigehito; Yoshida, Eiji
Synthetic Communications, 1996 , vol. 26, # 19 p. 3619 - 3626
反应条件
copper(I) sulphide; iron; potassium carbonate; dimethyl sulfoxide
T=110°C; 18 h; Inert atmosphere; chemoselective reaction;
参考文献
Wang, Huifeng; Jiang, Linlin; Chen, Tao; Li, Yarning
European Journal of Organic Chemistry, 2010 , # 12 p. 2324 - 2329
反应条件
copper(l) iodide; [DBU][HOAc]
T=130°C; 0.166667 h; Microwave irradiation;
参考文献
Singh, Neetu; Singh, Rahul; Raghuvanshi, Dushyant S.; Singh, Krishna Nand
Organic Letters, 2013 , vol. 15, # 22 p. 5874 - 5877
反应条件
hydrogenchloride; phenol in dichloromethane
T=0 - 25°C;
参考文献
Chasar, Dwight W.; Pratt, Timothy M.; Shockcor, J. P.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 183 - 186
反应条件
sodium trimethyl-silanolate in diethyl ether
T=-30°C;
参考文献
Effenberger, Franz; Russ, Werner
Chemische Berichte, 1982 , vol. 115, # 12 p. 3719 - 3736
反应条件
1: 1.0 mmol / potassium tert-butoxide / liquid ammonia / 2.5 h / -76 °C / Irradiation
2: 3.1 mmol / potassium tert-butoxide / dimethylsulfoxide / 15 h / 25 °C / Irradiation
3: 0.6 mmol / potassium tert-butoxide / dimethylformamide / 15 h / 25 °C / Irradiation
4: 73 percent / sodium isobutoxide / tetrakis(triphenylphosphine)palladium(0) / various solvent(s) / 8 h / Heating
View Scheme
参考文献
Cheng, Carlos; Stock, Leon M.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2436 - 2443
反应条件
AlCl3, aluminium chloride; thionyl chloride
T=70°C;
参考文献
Sun, Xiaoping; Haas, David; McWilliams, Samantha; Smith, Benjamin; Leaptrot, Katrina
Journal of Chemical Research, 2013 , vol. 37, # 12 p. 736 - 744
反应条件
AlCl3, aluminium chloride; thionyl chloride
T=-10°C; 1 h;
参考文献
Sun, Xiaoping; Haas, David; McWilliams, Samantha; Smith, Benjamin; Leaptrot, Katrina
Journal of Chemical Research, 2013 , vol. 37, # 12 p. 736 - 744
