in neat (no solvent) thermal decomposition at 260, 300, 340°C;
参考文献
Yudenich, S. G.; Druzhkov, O. N.; Uvarova, N. M.; Dodonov, V. A.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 2297 - 2301
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 2548 - 2552
in hexane
molar ratio of Al(C2H5)3 and Sb2O3 = 3 : 1, 60°C, 1 to 2 h; distn. in high vac.;
参考文献
Stamm,W.; Breindel,A.
Angewandte Chemie, 1964 , vol. 76, p. 99
Full Text Show Details
Stamm, W.
Trans. N. Y. Acad. Sci. (2), 1966 , vol. 28, p. 396 - 401
in neat (no solvent)
under N2; Al-compd. added slowly over a period of 2 h to Sb-compd. at 0°C with stirring, warmed slowly to room temp., stirred for 4 h, heated for 12 h at 120°C; monitored by NMR, fractional distn., Al-compd. isolated by distn.;;
参考文献
Thomas, C. J.; Krannich, L. K.; Watkins, C. L.
Polyhedron, 1993 , vol. 12, p. 89 - 94
