1H-imidazole; sodium hydride; lithium hexamethyldisilazane in tetrahydrofuran; hexane Ambient temperature;
参考文献
Barrett, Anthony G. M.; Morris, Timothy M.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2272 - 2277
1: carbonic acid dimethyl ester With sodium hydride in tetrahydrofuran; mineral oil T=65°C; 2: 7-methoxy-1-oxo-1,2,3,4-tetrahydronaphthalene in tetrahydrofuran; mineral oil T=65°C; 3.16667 h;
参考文献
Millennium Pharmaceuticals, Inc.
Patent: US2012/15942 A1, 2012 ;
Location in patent: Page/Page column 75 ;
US 20120015942 A1