T=69.9°C; P=750.06 Torr; 24 h; other conditions: reaction in the presence of CO2, labelling experiments, addition of <(PhCH2)NH3>Cl, other temperatures; MechanismProduct distribution;
hydroxylamine hydrochloride; potassium hydroxide in water
T=5°C; 8 h;
参考文献
Lajiness, James P.; Robertson, William M.; Dunwiddie, Irene; Broward, Melinda A.; Vielhauer, George A.; Weir, Scott J.; Boger, Dale L.
Journal of Medicinal Chemistry, 2010 , vol. 53, # 21 p. 7731 - 7738
potassium carbonate in N,N-dimethyl-formamide
T=130°C; 8 h; RefluxGreen chemistry;
参考文献
Jiang, Xinglong; Tiwari, Ashish; Thompson, Maethonia; Chen, Zhihong; Cleary, Thomas P.; Lee, Thomas B. K.
Organic Process Research and Development, 2001 , vol. 5, # 6 p. 604 - 608
potassium carbonate in N,N-dimethyl-formamide
T=130°C; 6 h; RefluxGreen chemistry;
参考文献
Jiang, Xinglong; Tiwari, Ashish; Thompson, Maethonia; Chen, Zhihong; Cleary, Thomas P.; Lee, Thomas B. K.
Organic Process Research and Development, 2001 , vol. 5, # 6 p. 604 - 608
