(S)-4-phenyl-1,4-diazalt;4.3.0gt;bicyclononane; diisobutylaluminium hydride; tin(ll) chloride in dichloromethane T=-100°C; 0.166667 h; Title compound not separated from byproducts;
(2,6-t-Bu2-4-Me-C6H2O)2AlMe; diisobutylaluminium hydride T=-78°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Maruoka, Keiji; Araki, Yoshitaka; Yamamoto, Hisashi
Journal of the American Chemical Society, 1988 , vol. 110, # 8 p. 2650 - 2652
1: With oxalyl dichloride in dichloromethane T=38°C; Vilsmeier-Haack reaction; 24 h; Inert atmosphere; 2: With sodium hydrogencarbonate in dichloromethane; water Inert atmosphere;
参考文献
Hassan, Jamal; Richards, Christopher J.
Synlett, 2012 , # 2 p. 239 - 242
