N,N-二乙基-邻甲基苯胺合成路线 （共 20 条）
反应条件
(CuOTf)2.C6H6 in tetrahydrofuran T=25°C; 1 h;
参考文献
Herman, Ashley M.; Johnson, Jeffrey S.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 219 - 224
反应条件
potassium hydroxide in dimethyl sulfoxide T=20 - 50°C;
参考文献
Zhang, Lei; Peng, Chen; Zhao, Dan; Wang, Yue; Fu, Hai-Jian; Shen, Qi; Li, Jian-Xin
Chemical Communications, 2012 , vol. 48, # 47 p. 5928 - 5930
反应条件
copper dichloride in tetrahydrofuran T=20°C; 0.25 h;
参考文献
Campbell, Matthew J.; Johnson, Jeffrey S.
Organic Letters, 2007 , vol. 9, # 8 p. 1521 - 1524
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; P=760.051 Torr; 24 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 2 p. 293 - 304
反应条件
PdCl2<(oTol)3P>2 in toluene T=100°C; 3 h;
参考文献
Kosugi, Masanori; Kameyama,Masayuki; Migita, Toshihiko
Chemistry Letters, 1983 , p. 927 - 928
反应条件
[RuIII(2,4-pentanedionato)3]; methanesulfonic acid; hydrogen; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=200°C; P=7500.75 Torr; 16 h; AutoclaveInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 19, # 33 p. 11039 - 11050
反应条件
methyl diphenyl silane; [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; sodium methylate in hexane T=60°C; 72 h; GloveboxSealed tube;
参考文献
Journal of the American Chemical Society, , vol. 135, # 4 p. 1248 - 1251
反应条件
sodium bromide T=175°C;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 3, p. 404
Chemische Berichte, , vol. 29, p. 1015
J.ind.eng.Chem., , vol. 13, p. 506
Chem. Zentralbl., , vol. 93, # I p. 18
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 20 °C 1.2: 8 h / 40 °C 2.1: [2,6-η6:η1-bis(2,4,6-trimethylphenyl)phenylthiolato]tris(4-fluorophenyl)phosphineruthenium(II)tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; sodium methylate; methyl diphenyl silane / hexane / 72 h / 60 °C / |Glovebox; |Sealed tube View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 4 p. 1248 - 1251
反应条件
in dichloromethane T=25°C; Yield given. Yields of byproduct given;
参考文献
Angewandte Chemie, , vol. 94, p. 711
