4-氨基-2-羟基苯甲酸乙酯合成路线 (共 9 条)
参考文献
Yale et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 1933,1934
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Anghel
Acad. Repub. Pop. Rom., Fil. Cluj, Stud. Cercet. Chim., 1956 , vol. 7, p. 151
Chem.Abstr., 1958 , p. 12801
反应条件
1: sulfuric acid / Diazotization.Eintragen der Diazoloesung in Jodwasserstoffsaeure und nachfolgendes Erwaermen auf 90grad 2: alcoholic NaOH-solution View Scheme
参考文献
Brenans; Prost
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1924 , vol. 178, p. 1011
反应条件
1.1: sulfuric acid / ethanol / 4 h / 50 °C / Inert atmosphere 2.1: potassium carbonate / acetone / 5 h / Reflux 3.1: water; sodium hydroxide / methanol / 2.5 h / Reflux 3.2: pH 7 View Scheme
参考文献
Terai, Takuya; Ito, Hiroki; Kikuchi, Kazuya; Nagano, Tetsuo
Chemistry - A European Journal, 2012 , vol. 18, # 24 p. 7377 - 7381
反应条件
sulfuric acid
6 h; Reflux;
参考文献
Terai, Takuya; Ito, Hiroki; Kikuchi, Kazuya; Nagano, Tetsuo
Chemistry - A European Journal, 2012 , vol. 18, # 24 p. 7377 - 7381
反应条件
2-methoxy-ethanol; platinum
Hydrogenation;
参考文献
Godtfredsen et al.
Acta Chemica Scandinavica (1947-1973), 1953 , vol. 7, p. 781,782
参考文献
Secareanu et al.
Acad. Repub. Pop. Rom., Fil. Cluj, Stud. Cercet. Chim., 1954 , vol. 5, p. 65,69, 70
Chem.Abstr., 1956 , p. 3314
参考文献
Rheinpreussen A.G.
Patent: DE846097 , 1949 ;
DRP/DRBP Org.Chem.
反应条件
1: nickel-aluminium-alloy; aq. NaOH solution
2: sulfuric acid
View Scheme
参考文献
Drain et al.
Journal of the Chemical Society, 1949 , p. 1498,1502
反应条件
2: platinum; 2-methoxy-ethanol / Hydrogenation
View Scheme
参考文献
Godtfredsen et al.
Acta Chemica Scandinavica (1947-1973), 1953 , vol. 7, p. 781,782