β-D-葡萄糖五乙酸酯合成路线 （共 318 条）
反应条件
indium tribromide in toluene
T=80°C; 0.0833333 h; optical yield given as percent de;
参考文献
Lefever, Mark R.; Szab, Lajos Z.; Anglin, Bobbi; Ferracane, Michael; Hogan, Joanna; Cooney, Lauren; Polt, Robin
Carbohydrate Research, 2012 , vol. 351, p. 121 - 125
反应条件
indium tribromide in 1,2-dichloro-ethane
T=80°C; 0.0833333 h; optical yield given as percent de;
参考文献
Lefever, Mark R.; Szab, Lajos Z.; Anglin, Bobbi; Ferracane, Michael; Hogan, Joanna; Cooney, Lauren; Polt, Robin
Carbohydrate Research, 2012 , vol. 351, p. 121 - 125
反应条件
1: 85 percent / PTSA / CHCl3 / 70 h / 90 °C
2: 94 percent / DBU / tetrahydrofuran / 22 h
View Scheme
参考文献
Ruttens, Bart; Van Der Eycken, Johan
Tetrahedron Letters, 2002 , vol. 43, # 12 p. 2215 - 2221
反应条件
phosphoric acid
T=120 - 130°C; P=30 Torr; 2 h;
参考文献
Novik, E. R.; Sokolov, V. M.; Studentsov, E. P.; Zakharov, V. I.; Lavrent'ev, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 1 p. 181 - 187,159 - 165
参考文献
Novik, E. R.; Sokolov, V. M.; Studentsov, E. P.; Zakharov, V. I.; Lavrent'ev, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 1 p. 181 - 187,159 - 165
反应条件
T=20 - 25°C; 0.75 h;
参考文献
Fernandez, Soledad; Crocamo, Nancy; Incerti, Marcelo; Giglio, Javier; Scarone, Laura; Rey, Ana
Journal of Labelled Compounds and Radiopharmaceuticals, 2012 , vol. 55, # 7 p. 274 - 280
反应条件
in diethyl ether
0.333333 h; Ambient temperature;
参考文献
Salinas, Amelia E.
Carbohydrate Research, 1999 , vol. 316, # 1-4 p. 34 - 46
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=20°C; 100 h;
参考文献
Petrovic, Zorica; Konstantinovic, Stanimir; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 1 p. 132 - 134
