2-己基-1,3-二噻戊环合成路线 （共 13 条）
反应条件
2,2'-azo-bisisobutyronitrile in neat (no solvent) T=80°C; 1.5 h; Product distribution;
参考文献
Gutierrez, Carlos G.; Stringham, Rex A.; Nitasaka, Tadashi; Glasscock, Karl G.
Journal of Organic Chemistry, 1980 , vol. 45, # 17 p. 3393 - 3395
反应条件
N-benzyl-DABCO tribromide in methanol; dichloromethane T=20°C; 0.1 h;
参考文献
Synthetic Communications, , vol. 36, # 8 p. 1093 - 1096
反应条件
(i) FSO3Me, CH2Cl2, (ii) /BRN= 1098229/; Multistep reaction;
参考文献
Corey,E.J.; Hase,T.
Tetrahedron Letters, 1975 , p. 3267 - 3268
反应条件
n-butyllithium in diethyl ether; hexane T=25°C; 4 h;
参考文献
Journal of the American Chemical Society, , vol. 102, # 10 p. 3577 - 3583
反应条件
in diethyl ether; hexane T=25°C; 4 h;
参考文献
Journal of the American Chemical Society, , vol. 102, # 10 p. 3577 - 3583
反应条件
2,2'-azo-bisisobutyronitrile in neat (no solvent) T=80°C; 1.5 h; Product distribution;
参考文献
Gutierrez, Carlos G.; Stringham, Rex A.; Nitasaka, Tadashi; Glasscock, Karl G.
Journal of Organic Chemistry, 1980 , vol. 45, # 17 p. 3393 - 3395
反应条件
thionyl chloride; silica gel in benzene
T=20°C; 5 h;
参考文献
Kamitori, Yasuhiro; Hojo, Masaru; Masuda, Ryoichi; Kimura, Tadashi; Yoshida, Tatsushi
Journal of Organic Chemistry, 1986 , vol. 51, # 9 p. 1427 - 1431
反应条件
2,4,6-trichloro-1,3,5-triazine; methoxymethoxy-propane in N,N-dimethyl-formamide
T=20°C; 0.75 h;
参考文献
Bandgar, Babasaheb P.; Joshi, Neeta S.; Bettigeri, Sampada V.
Monatshefte fur Chemie, 2007 , vol. 138, # 1 p. 67 - 71
反应条件
2,4,6-trichloro-1,3,5-triazine in N,N-dimethyl-formamide
T=20°C; 0.666667 h;
参考文献
Bandgar, Babasaheb P.; Joshi, Neeta S.; Bettigeri, Sampada V.
Monatshefte fur Chemie, 2007 , vol. 138, # 1 p. 67 - 71
反应条件
di-tert-butyl peroxide
T=150°C; 0.833333 h;
参考文献
Batyrbaev, N. A.; Zorin, V. V.; Zlot-skii, S. S.; Rakhmankulov, D. L.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1727 - 1729
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, p. 1934 - 1937
