2,3-二氢-2-苯基-4H-1-苯并噻喃-4-酮合成路线 （共 11 条）
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
P=1551.4 Torr; 15 h; Ambient temperature;
参考文献
Kumar; Rao; Pandey
Synthetic Communications, 1994 , vol. 24, # 22 p. 3297 - 3306
反应条件
phosphomolybdic acid supported on silica in ethanol
9.5 h; RefluxInert atmosphere;
参考文献
Sakirolla, Raghavendra; Yaeghoobi, Marzieh; Rahman, Noorsaadah Abd.
Monatshefte fur Chemie, 2012 , vol. 143, # 5 p. 797 - 800
反应条件
pyridine; lithium aluminium tetrahydride
T=25°C; 3.33333 h;
参考文献
Nakazumi, Hiroyuki; Ueyama, Tamio; Endo, Takashi; Kitao, Teijiro
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 4 p. 1251 - 1252
反应条件
aluminium trichloride in carbon disulfide
0.5 h; Heating; Yield given;
参考文献
Kaye; Mphahlele
Synthetic Communications, 1995 , vol. 25, # 10 p. 1495 - 1509
参考文献
Arndt
Chemische Berichte, 1923 , vol. 56, p. 1275
Chemische Berichte, 1925 , vol. 58, p. 1632
反应条件
1: hydrogen bromide; glacial acetic acid / 100 °C / im Rohr
2: phosphorus oxychloride
View Scheme
参考文献
Arndt
Chemische Berichte, 1923 , vol. 56, p. 1275
Chemische Berichte, 1925 , vol. 58, p. 1632
反应条件
1: hydrogen bromide; glacial acetic acid / 100 °C / im Rohr
2: phosphorus oxychloride
View Scheme
参考文献
Arndt
Chemische Berichte, 1923 , vol. 56, p. 1275
Chemische Berichte, 1925 , vol. 58, p. 1632
反应条件
trifluoromethanesulphinic acid in dichloromethane
9 h; Heatingother catalyst; other time; Product distributionMechanism;
参考文献
El-Zohry, M. F.; El-Khawaga, A. M.; Ismail, M. T.; Abdel-Wahab, A. A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 61, # 3.4 p. 373 - 380
反应条件
iodine in dimethyl sulfoxide
T=100°C; 18 h; further reagents DDQ, iodobenzene diacetate;
参考文献
Somogyi
Synthetic Communications, 1999 , vol. 29, # 11 p. 1857 - 1872
反应条件
sodium periodate in methanol; water
1.) 0 deg C, 3 h, 2.) r.t., 12 h;
参考文献
Somogyi, Laszlo
Liebigs Annalen der Chemie, 1994 , # 9 p. 959 - 960
