1: With tert.-butylhydroperoxide; (OC2H4)(OHC2H4)NC2H4N(C2H4OH)Cu(thiocyanate) in water; acetonitrile T=70°C; P=760.051 Torr; 2 h; 2: With triphenylphosphine in water; acetonitrile regioselective reaction;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 350, # 1-2 p. 26 - 34
hydrogenchloride; oxygen; sodium L-ascorbate; MnTPPCl in benzene Ambient temperaturepH=8.5, pO2= 1 atm; Further byproducts given. Title compound not separated from byproducts;
hydrogenchloride; oxygen; sodium L-ascorbate; MnTPPCl in benzene Ambient temperaturepH=8.5, pO2= 1 atm; Further byproducts given. Title compound not separated from byproducts;
